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Synthesis and properties of neptunium(VI,V) and plutonium(VI) pertechnetates

Fedosseev, A. M., Budantseva, N. A., Grigoriev, M. S., Guerman, K. E. and Krupa, J.-C.. "Synthesis and properties of neptunium(VI,V) and plutonium(VI) pertechnetates"

, vol. 91, no. 3, 2003, pp. 147-152.

Fedosseev, A., Budantseva, N., Grigoriev, M., Guerman, K. & Krupa, J. (2003). Synthesis and properties of neptunium(VI,V) and plutonium(VI) pertechnetates.

,

(3), 147-152.

Fedosseev, A., Budantseva, N., Grigoriev, M., Guerman, K. and Krupa, J. (2003) Synthesis and properties of neptunium(VI,V) and plutonium(VI) pertechnetates. Radiochimica Acta, Vol. 91 (Issue 3), pp. 147-152.

Fedosseev, A. M., Budantseva, N. A., Grigoriev, M. S., Guerman, K. E. and Krupa, J.-C.. "Synthesis and properties of neptunium(VI,V) and plutonium(VI) pertechnetates"

91, no. 3 (2003): 147-152.

Fedosseev A, Budantseva N, Grigoriev M, Guerman K, Krupa J. Synthesis and properties of neptunium(VI,V) and plutonium(VI) pertechnetates.

. 2003;91(3): 147-152.

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Preparation, crystal structure and properties revealed through IR and visible absorption spectroscopy study of Np(V,VI), Pu(VI) compounds formed with pertechnetate anions are reported. Spectrophotometric study of Np(V) and Pu(VI) in NH₄TcO₄ aqueous solutions (TcO₄^- concentration ranging between 0.2-0.5 M) shows only a slight interaction of NpO₂⁺ and PuO₂²⁺-ions with pertechnetate oxoanions in solution. On the contrary, for Np(V), Np(VI) and Pu(VI) pertechnetates in solid state, changes in the spectra clearly evidence the coordination of the actinides(V,VI) with TcO₄^--anions. That is in agreement with Np(VI) pertechnetate X-ray structural analysis performed on a single crystal.

Published Online: 2009-9-25

Published in Print: 2003-3-1

© 2003 Oldenbourg Wissenschaftsverlag GmbH

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