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JP2012201679A - Method of simultaneous straightening and dyeing of frizzy hair

JP2012201679A - Method of simultaneous straightening and dyeing of frizzy hair - Google PatentsMethod of simultaneous straightening and dyeing of frizzy hair Download PDF Info
Publication number
JP2012201679A
JP2012201679A JP2011087719A JP2011087719A JP2012201679A JP 2012201679 A JP2012201679 A JP 2012201679A JP 2011087719 A JP2011087719 A JP 2011087719A JP 2011087719 A JP2011087719 A JP 2011087719A JP 2012201679 A JP2012201679 A JP 2012201679A
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hair
dye
agent
straightening
dyeing
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2011-03-25
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Japanese (ja)
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Genichiro Okuyama
源一郎 奥山
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Individual
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2011-03-25
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2012-10-22
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2011-03-25 Priority to JP2011087719A priority Critical patent/JP2012201679A/en
2012-10-22 Publication of JP2012201679A publication Critical patent/JP2012201679A/en
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PROBLEM TO BE SOLVED: To provide a method of reducing the damage to the hair and the burden on the clients in terms of time and expense by making straightening and dyeing of frizzy hairs simultaneously.SOLUTION: The method of simultaneous straightening and dyeing of frizzy hairs comprises applying a reductant containing not less than 3% and not more than 10% of cysteamine hydrochloride or 1-thioglycerol to frizzy hairs, rinsing them, straightening the frizzy hairs with a frizzy hair straightening iron, oxidizing them with a mixture of the first agent of a hair color containing an oxidation dye and the second agent of the hair color containing hydrogen peroxide so that the frizzy hairs are straightened and dyed simultaneously. Preferably the hydrogen peroxide concentration in the mixture of the first agent of the hair color and the second agent of the other hair color is not less than 3% and not more than 6%.

Description Translated from Japanese

本発明は縮毛を直毛に矯正すると同時に染毛する方法に関する。The present invention relates to a method for correcting curly hair to straight hair and simultaneously dyeing the hair.

黄色人種の７割が癖毛であるといわれており特に女性は髪がもつれ朝の手入れが大変、ヘアースタイルが決まらない等の悩みを抱えており美容上の大きな問題になっている。
また女性の７０％が白髪染めまたはおしゃれ染めで毛髪を染めている。
従来縮毛矯正にはチオグリコール酸塩を含有した医薬部外品の縮毛矯正剤と高温の縮毛矯正用アイロンを使用した施術法が汎用されている。一方染毛には酸化染料を含有した医薬部外品の染毛剤第一剤と過酸化水素水を含有した医薬部外品の染毛剤第二剤を１：１で混合し毛髪に塗布し染毛する方法が使用されている。
縮毛矯正も染毛も毛髪をいためるため１週間以上間隔をあけて施術するように行政指導（薬発３７６号：厚生省薬務局長通知）されているため 消費者は二度美容院に行かなければならず、時間と経費がかかるため負担がおおきい。It is said that 70% of the yellow race is eyelashes, and especially women have troubles such as hair tangles that are difficult to care for in the morning, and hair styles are not determined, which is a major cosmetic problem.
In addition, 70% of women have their hair dyed with gray hair or fashion dye.
Conventionally, a treatment method using a quasi-drug curative straightener containing thioglycolate and a high-temperature curly straightening iron is widely used for straightening hair. On the other hand, for hair dye, a quasi-drug hair dye first agent containing an oxidative dye and a quasi-drug hair dye second agent containing hydrogen peroxide water were mixed at a ratio of 1: 1 and applied to the hair. Hair dyeing methods are used.
Because of the administrative guidance (Yakuhaku No. 376: Notification of the Director of Pharmacy, Ministry of Health and Welfare) that the hair is curled and dyed in order to heal the hair, the consumer must go to the beauty salon twice. This is expensive and time consuming and expensive.

従来縮毛の矯正にはチオグリコール酸アンモニウムを含有する医薬部外品の縮毛矯正剤を縮毛に塗布し２０−４０分ほど放置し毛髪を還元後 水洗し 摂氏１８０度という高温の縮毛矯正用アイロンを使用し高熱で毛髪を熱変性させながら毛髪を伸ばし、その後酸化剤で毛髪を酸化し水洗後仕上げる縮毛矯正法が汎用されている。Conventionally, for curly hair correction, a quasi-drug curative containing ammonium thioglycolate is applied to the curly hair, left for about 20-40 minutes, the hair is reduced, washed with water, and heated at a high temperature of 180 degrees Celsius. A hair straightening method is widely used in which a straightening iron is used to stretch the hair while heat-denaturing the hair with high heat, and then the hair is oxidized with an oxidizing agent and then washed and washed.

一方日本女性の約７０％が医薬部外品の染毛剤で毛染めをしている。染毛剤は酸化染料を含有する染毛剤第一剤と過酸化水素を含有する染毛剤第二剤を１：１で混合し毛髪に塗布後約２０−３０分放置し毛髪を染毛する。On the other hand, about 70% of Japanese women dye their hair with quasi-drug hair dyes. For the hair dye, the first hair dye containing an oxidative dye and the second hair dye containing hydrogen peroxide are mixed at a ratio of 1: 1 and applied to the hair, and then left for about 20-30 minutes to dye the hair. To do.

縮毛矯正の過程では第一剤のチオグリコール酸塩による毛髪の還元の工程と第二剤のブロム酸塩または過酸化水素による酸化工程により毛髪はダメージする。染毛の工程ではアンモニア水を含む第一剤と過酸化水素水を含む第二剤の混合物を毛髪に塗布するため毛髪をダメージする。
つまり縮毛矯正と染毛を行うには毛髪の還元、毛髪の酸化、毛髪の染毛の３工程が必要である。
この二つの美容技術はともに毛髪をいためるため、毛髪のダメージを少しでも抑えるためそれぞれを１週間以上の期間をあけて施術するよう行政指導されている。In the process of straightening hair, the hair is damaged by the process of reducing hair with thioglycolate as the first agent and the oxidation process with bromate or hydrogen peroxide as the second agent. In the hair dyeing process, hair is damaged because a mixture of the first agent containing ammonia water and the second agent containing hydrogen peroxide solution is applied to the hair.
In other words, three steps of hair reduction, hair oxidation, and hair dyeing are required for straightening and dyeing hair.
These two beauty techniques are both administratively instructed to treat each hair with a period of one week or longer in order to curb hair, and to prevent any damage to the hair.

縮毛の矯正と染毛を行うために消費者はのべ約５時間、二日にわけて美容院に行かねばならず さらに個別の美容施術を受けるため経費も二倍かかり時間的にも経済的にも負担が大きい。
縮毛矯正と染毛の二つの美容施術を一回で同時に行う施術方法の開発が望まれていた。In order to correct hair and correct hair, consumers have to go to the beauty salon for about 5 hours in total, and to take individual beauty treatments, it costs twice as much and is economical in terms of time. The burden is large.
There has been a demand for the development of a treatment method that simultaneously performs two cosmetic treatments of curly hair straightening and dyeing.

縮毛矯正は毛髪との接触面が１８０度にもなる縮毛矯正用アイロンを使用し還元された毛髪を少しずつアイロンの加熱面ではさんで伸ばすため施術時間がかかり３時間以上の場合も少なくない。
一方染毛は染毛剤第一剤と染毛剤第二剤を混合し毛髪に塗布後２０−３０分放置しシャンプー後乾燥し仕上げる。その施術時間は２時間ほどである。
消費者はこの二つの施術を続けて行うことが毛髪のダメージが大きく行政により規制されているため１週間以上 間隔をあけ二日に分けて美容院に行かねばならず美容院での技術料もそれぞれの技術に支払うため時間的経済的に負担が大きい。
１日で縮毛を矯正すると同時に染毛できる毛髪へのダメージの少ない縮毛矯正同時染毛方法の開発が望まれている。Hair straightening uses a hair straightening iron with a contact surface as much as 180 degrees, and the reduced hair is stretched between the iron heating surfaces little by little. Absent.
On the other hand, for hair dyeing, the first hair dye and the second hair dye are mixed, applied to the hair, left for 20-30 minutes, dried after shampooing and finished. The treatment time is about 2 hours.
Consumers are required to go to the beauty salon at least one week apart for two days because the hair damage is severely regulated by the government to continue these two treatments. Because of paying for each technology, there is a heavy time and cost burden.
It is desired to develop a method for simultaneously dyeing curly hair that corrects curly hair in one day and that can simultaneously dye hair with little damage to the hair.

課題を解決する為の手段Means to solve the problem

本発明者は鋭意研究の結果 還元剤としてシステアミン塩酸塩または１−チオグリセロールを含む薬剤を毛髪に塗布し自然放置し水洗後、縮毛矯正用ヘアーアイロンで癖毛を直毛に伸ばし そのあとで染毛剤一剤と染毛剤二剤の混合液を塗布し、染毛すると同時に還元剤で還元された毛髪を酸化固定し直毛にする縮毛矯正同時染毛方法を完成した。
つまり従来の毛髪の還元工程、毛髪の酸化工程、染毛工程の３工程に替わり、本発明では毛髪の還元工程、染毛剤による酸化工程の２工程により縮毛矯正と染毛を行うことができることを考案し本発明を完成した。
本発明による毛髪のダメージの軽減効果、ならびに時間的経済的負担軽減は大変大きい。As a result of diligent research, the present inventor applied a drug containing cysteamine hydrochloride or 1-thioglycerol as a reducing agent to the hair, left to stand naturally, washed with water, then straightened the eyelashes with a curling hair straightener, and then A mixed solution of one hair dye and two hair dyes was applied to complete the curly straightening simultaneous hair dyeing method in which hair was dyed at the same time and the hair reduced by the reducing agent was oxidized and fixed to straight hair.
In other words, instead of the conventional hair reduction process, hair oxidation process, and hair dyeing process, in the present invention, the hair reduction process and the hair dyeing process can be performed in two steps: hair reduction and hair dyeing. We have devised what we can do to complete the present invention.
The effect of reducing hair damage and reducing the time and economic burden according to the present invention are very large.

染毛剤第一剤と染毛剤第二剤の混合物に含まれる過酸化水素の濃度は染毛剤第一剤に配合された酸化染料を酸化重合すると同時に還元剤で還元された毛髪を酸化固定するために３％以上６％以下が望ましいが毛髪のダメージの度合いによりこの範囲だけではない。The concentration of hydrogen peroxide contained in the mixture of the first hair dye and the second hair dye oxidizes and polymerizes the oxidized dye contained in the first hair dye and simultaneously oxidizes the hair reduced by the reducing agent. In order to fix, 3% or more and 6% or less are desirable, but it is not limited to this range depending on the degree of hair damage.

さらに還元剤であるシステアミン塩酸塩又は１−チオグリセロールを塗布後と水洗後に摂氏３７度の発熱キャップ（特許公開広報 ２００８−２３７６８１）を被り毛髪を数十分保温することによりまた水洗後さらに数十分発熱キャップを被ることより縮毛矯正用ヘアーアイロンを使用したときの縮毛の伸びがよく容易に直毛となることを発見した。さらに染毛時に発熱キャップを被ることにより染毛が均一で 短時間にできることを発見した。Furthermore, after applying cysteamine hydrochloride or 1-thioglycerol, which is a reducing agent, and after washing with water, a heat cap of 37 degrees Celsius (Patent Publication 2008-237681) is put on and the hair is kept warm for several tens of minutes. It was discovered that the curly hair stretched easily when using a curling hair straightener, and it became straight hair easily by wearing a partial fever cap. Furthermore, it was discovered that by covering the heat generating cap at the time of hair dyeing, the hair can be made uniformly and in a short time.

発明の効果Effect of the invention

還元剤としてシステアミン塩酸塩または１−チオグリセロールを含む薬剤を毛髪に塗布し自然放置した後 高温の縮毛矯正用ヘアーアイロンを使用し縮毛を直毛に伸ばしたあとで染毛剤一剤と染毛剤二剤の混合液を塗布し、染毛すると同時に還元剤で還元された縮毛を酸化し直毛にする縮毛矯正と同時に染毛する方法開発した。従来は５時間近くのべ二日かかっていた美容院での縮毛矯正と染毛の施術を一日、３−４時間で行うことができ、その時間的 経済的負担軽減は大変大きい。
つまり本発明は 縮毛矯正と染毛を同時に行う方法であり消費者の毛髪ダメージの軽減と時間的負担の軽減、経済的負担の軽減を実現した美容方法でありその消費者に与えるメリットは絶大である。After applying a medicine containing cysteamine hydrochloride or 1-thioglycerol as a reducing agent to the hair and leaving it to stand, use a high temperature curling hair curling iron to straighten the hair to a straight hair A mixed solution of two hair dyes was applied to the hair, and at the same time, a method for dyeing hair simultaneously with curly hair straightening was developed. Hairdressing and hair dyeing at a beauty salon, which previously took nearly two hours for nearly five hours, can be performed in 3-4 hours a day, which greatly reduces the time and economic burden.
In other words, the present invention is a method of performing curly hair straightening and hair dyeing simultaneously, and is a beauty method that realizes reduction of consumer hair damage, reduction of time burden, and reduction of economic burden. It is.

発明の実施の為の最良の方法Best Mode for Carrying Out the Invention

以下本発明の実施の形態を説明する。
本発明に使用するシステアミン塩酸塩とはＣＡＳ Ｎｏ．１５６−５７−０、１−チオグリセロールとはＣＡＳ Ｎｏ．９６−２７−５で規定される物質であり分子内にチオール基を持つため還元作用がある。Embodiments of the present invention will be described below.
The cysteamine hydrochloride used in the present invention is CAS No. 156-57-0, 1-thioglycerol means CAS No. It is a substance defined by 96-27-5 and has a reducing action because it has a thiol group in the molecule.

システアミン塩酸塩、又は１−チオグリセロールを３−１０重量％含有する粘度３０００−５００００ＣＰＳの還元剤を調整する。A reducing agent having a viscosity of 3000-50000 CPS containing 3-10% by weight of cysteamine hydrochloride or 1-thioglycerol is prepared.

一方酸化染料を含有する染毛剤第一剤と過酸化水素を含有する染毛剤第二剤を調製する。染毛剤第一剤に配合される染毛剤の酸化染料ならびに有効成分は次のものが上げられこれらから数種類の酸化染料ならびに有効成分が処方配合される。
５−アミノオルトクレゾール、２−アミノー４−ニトロフェノール、２−アミノー５ニトロフェノール、１−アミノー４メチルアミノアントラキノン、３，３イミノジフェノール、塩酸２，４−ジアミノフェノキシエタノール、塩酸２，４−ジアミノフェノール、塩酸トルエン２，５ジアミン、塩酸パラニトロフェニレンジアミン、塩酸パラフェニレンジアミン、塩酸Ｎ−フェニルパラフェニレンジアミン、塩酸メタフェニレンジアミン、オルトアミノフェノール、酢酸Ｎ−フェニルパラフェニレンジアミン、１，４−ジアミノアントラキノン、２，６−ジアミノピリジン、１，５−ジヒドロキシナフタレン、トルエン２，６−ジアミン、トルエン３，４−ジアミン、ニトロパラフェニレンジアミン、パラアミノフェノール、パラニトロオルトフェニレンジアミン、パラフェニレンジアミン、パラメチルアミノフェノール、ピクラミン酸、ピクラミン酸ナトリウム、Ｎ，Ｎ−ビス（４−アミノフェニル）２，５、ジアミノー１，４−キノンジイミン、５−（２−ヒドロキシアミノ）−２−メチルフェノール、ｎ−フェニルパラフェニレンジアミン、メタアミノフェノール、

フェノール、硫酸オルトアミノフェノール、硫酸オルトクロルパラフェニレンジアミン 硫酸４，４−ジアミノジフェニルアミン、硫酸２，４−ジアミノフェノール、硫酸トルエンー２、５−ジアミン、硫酸ニトロパラフェニレンジアミン、硫酸ニトロパラフェニレンジアミン、硫酸パラアミノフェノール、硫酸パラニトロオルトフェニレンジアミン、硫酸パラニトロメタフェニレンジアミン、硫酸パラメチルアミノフェノール、硫酸メタアミノフェノール、硫酸メタフェニレンジアミン、カテコール、ヒドロキノン、ピロガロール、フロログリシン、没食子酸、レゾルシン
染毛剤第二剤には過酸化水素が配合され日本の薬事法では配合濃度の上限は６％である。On the other hand, a hair dye first agent containing an oxidative dye and a hair dye second agent containing hydrogen peroxide are prepared. The following are the oxidation dyes and active ingredients of the hair dye to be blended in the first hair dye, and several kinds of oxidation dyes and active ingredients are formulated and blended.
5-aminoorthocresol, 2-amino-4-nitrophenol, 2-amino-5nitrophenol, 1-amino-4-methylaminoanthraquinone, 3,3-iminodiphenol, 2,4-diaminophenoxyethanol hydrochloride, 2,4-diamino hydrochloride Phenol, toluene 2,5 diamine hydrochloride, paranitrophenylenediamine hydrochloride, paraphenylenediamine hydrochloride, N-phenylparaphenylenediamine hydrochloride, metaphenylenediamine hydrochloride, orthoaminophenol, N-phenylparaphenylenediamine acetate, 1,4-diamino Anthraquinone, 2,6-diaminopyridine, 1,5-dihydroxynaphthalene, toluene 2,6-diamine, toluene 3,4-diamine, nitroparaphenylenediamine, paraaminophenol, paranitrool Phenylenediamine, paraphenylenediamine, paramethylaminophenol, picramic acid, sodium picramate, N, N-bis (4-aminophenyl) 2,5, diamino-1,4-quinonediimine, 5- (2-hydroxyamino)- 2-methylphenol, n-phenylparaphenylenediamine, metaaminophenol,
Phenol, orthoaminophenol sulfate, orthochloroparaphenylenediamine sulfate 4,4-diaminodiphenylamine sulfate, 2,4-diaminophenol sulfate, toluene-2,5-diamine sulfate, nitroparaphenylenediamine sulfate, nitroparaphenylenediamine sulfate, sulfuric acid Paraaminophenol, paranitroorthophenylenediamine sulfate, paranitrometaphenylenediamine sulfate, paramethylaminophenol sulfate, metaaminophenol sulfate, metaphenylenediamine sulfate, catechol, hydroquinone, pyrogallol, phloroglysin, gallic acid, resorcin hair dye Hydrogen peroxide is blended into the two agents, and the upper limit of the blending concentration is 6% according to the Japanese Pharmaceutical Affairs Law.

縮毛に還元剤含む製剤を塗布し１５−３０分室温で放置。水洗し還元剤を除去する。水洗後タオルドライし縮毛矯正用ヘアーアイロンで癖毛を伸ばし直毛に矯正する。
その後染毛剤第一剤と染毛剤第二剤を混合した混合液を塗布し２０分放置し染毛すると同時に還元剤で還元された毛髪を酸化し縮毛矯正を完成する。Apply a formulation containing a reducing agent to curly hair and leave at room temperature for 15-30 minutes. Wash with water to remove the reducing agent. After washing with water, dry the towel and straighten the eyelashes with a curling hair straightener.
Thereafter, a mixed solution in which the first hair dye agent and the second hair dye agent are mixed is applied and left for 20 minutes to dye the hair. At the same time, the hair reduced by the reducing agent is oxidized to complete the curly hair correction.

縮毛矯正効果と染毛剤の効果をさらに高めるためには、縮毛に還元剤を塗布したあと１５分程度３７度で発熱キャップを被り保温放置し還元を充分に行い水洗し還元剤を除去した後さらに３７度で発熱キャップを被り１５分保温放置し縮毛矯正用ヘアーアイロンで縮毛を伸ばし直毛に矯正する。
さらに染毛剤第一剤と染毛剤第二剤混合物を頭髪に塗布し発熱キャップを被り３７度で１０分放置し染毛同時に毛髪に浸透した還元剤を酸化し水洗し仕上げる。To further improve the curly hair straightening effect and hair dyeing effect, apply a reducing agent to the curly hair and cover it with a heat-generating cap at 37 degrees for about 15 minutes. After that, it is further covered with a heat generating cap at 37 ° C. and left for 15 minutes, and the curly hair is straightened and straightened with a curling hair straightener.
Further, the hair dye first agent and the hair dye second agent mixture are applied to the hair, covered with a heat generating cap, left at 37 ° C. for 10 minutes, and the reducing agent that has penetrated into the hair simultaneously with the hair is oxidized and washed with water.

以下例よって具体的に説明する。
還元剤を含む処方例１，２，３， 酸化剤ならびに染毛剤第一剤、染毛剤第二剤の処方例、調整法は次の通りである。

資料調整の方法）A specific example will be described below.
Formulation examples 1, 2 and 3, including a reducing agent, formulation examples and preparation methods for the oxidizing agent, the first hair dye, and the second hair dye are as follows.
How to adjust materials)

還元剤の調整方法： （処方例１，２，３ ）
１）成分１，２，３をビーカーに取り摂氏８０度で溶解する。
２）成分９をビーカーに取り摂氏８０度で溶解する。
２）に１）を攪拌機で攪拌しながら投入混合し５分間攪拌し乳化する。
摂氏５０度で成分４，５，６，７，８、を混合物に投入し混合物を摂氏３５度まで冷却 し資料とする。Adjustment method of reducing agent: (Prescription Examples 1, 2, 3)
1) Take ingredients 1, 2, and 3 in a beaker and dissolve at 80 degrees Celsius.
2) Take component 9 in a beaker and dissolve at 80 degrees Celsius.
Add 1) to 2) while stirring with a stirrer and stir for 5 minutes to emulsify.
Add ingredients 4, 5, 6, 7, and 8 to the mixture at 50 degrees Celsius, cool the mixture to 35 degrees Celsius, and use the data.

染毛剤第一剤の調製方法（処方例４）
１）成分１２，１３，１４をビーカーに取り摂氏８０度で溶解する。
２）成分１０，１１，１５，１７をビーカーに取り摂氏８０度で溶解する。
２）に１）を攪拌機で攪拌しながら投入混合し５分間攪拌し乳化する。
摂氏５０度で成分１６を投入し混合物を摂氏３５度まで攪拌冷却し資料とする。Preparation method of hair dye first agent (formulation example 4)
1) Take ingredients 12, 13, and 14 in a beaker and dissolve at 80 degrees Celsius.
2) Take ingredients 10, 11, 15, and 17 in a beaker and dissolve at 80 degrees Celsius.
Add 1) to 2) while stirring with a stirrer and stir for 5 minutes to emulsify.
Ingredient 16 is charged at 50 degrees Celsius, and the mixture is stirred and cooled to 35 degrees Celsius for use as data.

染毛剤第二剤の調製方法（処方例５，６）
１）成分２０，２１，２２をビーカーに取り摂氏８０度で溶解する。
２）成分１９，２３をビーカーに取り摂氏８０度で溶解する。
２）に１）を攪拌機で攪拌しながら投入混合し５分間攪拌し乳化する。
混合物に摂氏５０度で成分１８を投入しさらに混合物を攪拌し資料とする。Preparation method of hair dye second agent (Prescription Examples 5 and 6)
1) Take ingredients 20, 21, 22 in a beaker and dissolve at 80 degrees Celsius.
2) Take ingredients 19 and 23 in a beaker and dissolve at 80 degrees Celsius.
Add 1) to 2) while stirring with a stirrer and stir for 5 minutes to emulsify.
Ingredient 18 is added to the mixture at 50 degrees Celsius, and the mixture is further stirred to prepare a document.

酸化剤の調製方法（処方例７）
１）成分２７，２８，２９をビーカーに取り摂氏８０度で溶解する。
２）成分２５，２６，２７，２８，２９をビーカーに取り摂氏８０度で溶解する。
２）に１）を攪拌機で攪拌しながら投入混合し５分間攪拌し乳化する。
摂氏５０度で成分２４を投入し混合物を摂氏３５度まで冷却し資料とする。
効果の測定）Preparation method of oxidizing agent (formulation example 7)
1) Take ingredients 27, 28 and 29 in a beaker and dissolve at 80 degrees Celsius.
2) Take components 25, 26, 27, 28, and 29 in a beaker and dissolve at 80 degrees Celsius.
Add 1) to 2) while stirring with a stirrer and stir for 5 minutes to emulsify.
Ingredient 24 is charged at 50 degrees Celsius, and the mixture is cooled to 35 degrees Celsius and used as data.
Effect measurement)

実施例１
かつて縮毛矯正アイロンによる縮毛矯正をした事のある縮毛で白髪のある女性１に処方例１のクリーム状の還元剤を塗布し２５分放置した。毛髪の軟化を確認し水洗後タオルドライし縮毛矯正用ヘアーアイロンで縮毛を伸ばした。その後頭髪を左右に分け右に処方例４の染毛剤第一剤１０ｇと処方例５の染毛剤第二剤５０ｇを混合した染毛剤を左に、処方例４の染毛剤第一剤１０ｇと処方例６の染毛剤第二剤５０ｇを混合した混合物を塗布し２０分放置後シャンプーしブローし仕上げた。
トータルの施術時間は３時間であったExample 1
The creamy reducing agent of Formulation Example 1 was applied to a woman 1 with curly hair that had been hair straightened with a hair straightening iron and left for 25 minutes. After confirming softening of the hair, it was washed with water and dried with a hair iron for straightening hair. Thereafter, the hair is divided into right and left, and on the right, the hair dye obtained by mixing 10 g of the hair dye first agent of the prescription example 4 and 50 g of the hair dye second agent of the prescription example 5 is on the left. A mixture of 10 g of the agent and 50 g of the hair dye second agent of Formulation Example 6 was applied, left for 20 minutes, then shampooed and blown to finish.
Total treatment time was 3 hours

実施例２
かつて縮毛矯正用アイロンによる縮毛矯正をした事のある縮毛で白髪のある女性２に処方例１のクリーム状の還元剤を塗布し３７度の発熱キャップを被り１５分放置した。毛髪の軟化を確認し水洗後再度３７度の発熱キャップを被り１５分放置した。キャップをはずし縮毛矯正用ヘアーアイロンで縮毛矯正した。その後頭髪を左右に分け右に処方例４の染毛剤第一剤１０ｇと処方例５の染毛剤第二剤５０ｇの混合物６０ｇを左に染毛剤第一剤１０ｇと処方例６の染毛剤第二剤５０ｇを混合した混合物６０ｇを塗布し２０分放置後シャンプーしブローし仕上げた。
縮毛矯正と白髪染めのトータルの施術時間は３時間半であり一日で終了した。Example 2
The creamy reducing agent of Formulation Example 1 was applied to a woman 2 with curly and gray hair that had been hair straightened with a hair straightening iron once, covered with a 37 ° exothermic cap and left for 15 minutes. After confirming the softening of the hair, it was washed with water and again covered with a 37 ° exothermic cap and left for 15 minutes. The cap was removed and the hair was straightened with a hair iron for straightening hair. Thereafter, the hair is divided into right and left, 60 g of a mixture of 10 g of the hair dye first agent of Formulation Example 4 and 50 g of the hair dye second agent of Formulation Example 5 on the right, and 10 g of the hair dye first agent and Dye of Formulation Example 6 on the left. 60 g of a mixture containing 50 g of the hair second agent was applied, left for 20 minutes, then shampooed and blown to finish.
The total treatment time for curly hair straightening and white hair dyeing was 3.5 hours, and it was completed in one day.

比較例１
かつて縮毛矯正用アイロンによる縮毛矯正をした事のある縮毛で白髪のある女性３に処方例３のクリーム状の還元剤８０ｇを塗布し２５分放置した。毛髪の軟化を確認後水洗しタオルドライ後 縮毛矯正用のアイロンを使用し２時間かけて宿毛を伸ばした。その後頭髪に処方例７の酸化剤８０ｇ塗布し２０分放置後シャンプーしブローし仕上げた。トータルの施術時間は３時間かかった。
１週間後再度美容院を訪れ処方例４の染毛剤第一剤６０ｇと処方例５の染毛剤第二剤６０ｇの混合物１２０ｇを頭髪に塗布し白髪染めを行った。施術時間は１時間半であった。
縮毛矯正と白髪染めのトータル時間は４時間半であり延べ日数は２日であった。Comparative Example 1
80 g of the cream-like reducing agent of Formulation Example 3 was applied to a woman 3 with curly and gray hair that had been straightened with a hair straightening iron once and left for 25 minutes. After confirming the softening of the hair, it was washed with water and dried with a towel. The hair was stretched for 2 hours using a hair straightening iron. Thereafter, 80 g of the oxidizing agent of Formulation Example 7 was applied to the hair, left for 20 minutes, then shampooed and blown to finish. Total treatment time took 3 hours.
One week later, the hair salon was visited again, and 120 g of a mixture of 60 g of the hair dye first agent of Prescription Example 4 and 60 g of the hair dye second agent of Prescription Example 5 was applied to the hair and dyed gray hair. The treatment time was one and a half hours.
The total time for straightening hair and dyeing white hair was 4 hours and a half, and the total number of days was 2 days.

実施例１、実施例２、比較例１それぞれに毛量、毛質のほぼ同じ３名の女性をモデルとし、本人と美容師３名による効果の測定のためアンケートを実施した。
アンケートの項目ならびに配点は以下の通りである。
評価基準
大変良い ５点
良い ４点
普通 ３点
悪い ２点
大変悪い １点Each of Example 1, Example 2, and Comparative Example 1 was modeled on three women with almost the same amount of hair and hair, and a questionnaire was conducted to measure the effects of the person and three hairdressers.
The questionnaire items and points are as follows.
Evaluation criteria Very good 5 points 4 points normal 3 points bad 2 points very bad 1 point

結果は下記の通りである。
モデルの女性３名による自己評価結果
評価点はそれぞれのモデルの評価点
評価結果 実施例１の左 同右 実施例２の左 同右 比較例１
施術時間（縮毛矯正＋染毛） ５ ５ ４ ４ １
髪のダメージ ４ ４ ４ ４ ２
ボリュームダウン ５ ５ ５ ５ ５
手触り ４ ４ ５ ５ ３
白髪の染まり ５ ４ ５ ５ ４
一ヵ月後のダメージ ４ ４ ４ ４ ２
一ヵ月後の手触り ４ ４ ５ ５ ２
一ヵ月後の白髪の染まり ５ ４ ５ ５ ３
朝の手入れのしやすさ ４ ４ ５ ５ ４
満足度 ４ ４ ５ ４ ２The results are as follows.
The self-evaluation result evaluation score by three women of the model is the evaluation score evaluation result of each model. Left of Example 1 Same as the left Example 2 Left Same as the right Comparative Example 1
Treatment time (hair straightening + hair dyeing) 5 5 4 4 1
Hair damage 4 4 4 4 2
Volume down 5 5 5 5 5
Touch 4 4 5 5 3
Dyeing gray hair 5 4 5 5 4
Damage after one month 4 4 4 4 2
Touch after one month 4 4 5 5 2
The color of gray hair one month later 5 4 5 5 3
Ease of morning care 4 4 5 5 4
Satisfaction 4 4 5 4 2

美容師３名による評価
点数は３人の平均値を四捨五入し整数にしたものである。
評価結果 実施例１の左 同右 実施例２の左 同右 比較例１
施術時間（縮毛矯正＋毛染め） ５ ５ ４ ４ １
髪のダメージ ５ ４ ５ ４ ４
ボリュームダウン ５ ５ ５ ５ ５
手触り ４ ４ ５ ５ ４
白髪の染まり ４ ４ ５ ５ ３
一ヵ月後のダメージ ４ ４ ５ ５ ２
一ヵ月後の手触り ４ ４ ５ ５ ２
一ヵ月後の白髪の染まり ４ ４ ５ ５ ３
満足度 ４ ４ ５ ５ ２The evaluation score by three hairdressers is the average value of three people rounded to an integer.
Evaluation result Left of Example 1 Same as right Left of Example 2 Same as right Comparative example 1
Treatment time (hair straightening + hair dyeing) 5 5 4 4 1
Hair damage 5 4 5 4 4
Volume down 5 5 5 5 5
Touch 4 4 5 5 4
Dyeing gray hair 4 4 5 5 3
Damage after one month 4 4 5 5 2
Touch after one month 4 4 5 5 2
Dyeing of gray hair one month later 4 4 5 5 3
Satisfaction 4 4 5 5 2

以上の結果 実施例１，２で示したごとく本発明の縮毛矯正と染毛を同時に行う方法は従来の縮毛矯正したあと、１週間あけて染毛する方法に比べ毛髪のダメージが少なく、トータルな施術時間が少なく消費者の満足度が従来の二日にわたる施術法に比べ遥かに大きいことが確認できた。
本発明において、過酸化水素は染毛剤の染料の酸化重合と還元剤であるシステアミン塩酸塩、または１−チオグリセロールによって還元された毛髪の酸化にともに消費される。
過酸化水素の配合量は多いほうが良く染毛剤第一剤、第二剤混合時の濃度は３−６％がよい。
さらに請求項２で請求した染毛剤一剤 二剤の混合時の過酸化水素濃度を３−６％にすることにより、還元剤の酸化に使われる過酸化水素と染毛剤第一剤の染料の酸化重合に消費される過酸化水素を充分にまかなうことができ縮毛矯正と染毛を同時にできることが確認された。
さらに請求項３で請求したように発熱キャップを被ることにより、縮毛矯正時の反応を早め美しい仕上がりと染毛剤の色持ち効果が長持ちすることが確認された。The above results As shown in Examples 1 and 2, the method of simultaneously performing hair straightening and hair dyeing of the present invention has less hair damage compared to the conventional method of straightening hair after one week of hair straightening, It was confirmed that the total treatment time was short and the satisfaction level of consumers was much higher than the conventional two-day treatment method.
In the present invention, hydrogen peroxide is consumed together with the oxidative polymerization of the dye of the hair dye and the oxidation of the hair reduced by cysteamine hydrochloride, which is the reducing agent, or 1-thioglycerol.
A larger amount of hydrogen peroxide is better, and the concentration when the hair dye first agent and second agent are mixed is preferably 3-6%.
Furthermore, by setting the hydrogen peroxide concentration at the time of mixing the two hair dyes in claim 2 to 3-6%, the hydrogen peroxide used for the oxidation of the reducing agent and the first hair dye agent It was confirmed that the hydrogen peroxide consumed for the oxidative polymerization of the dye can be adequately covered, and that hair straightening and hair dyeing can be performed simultaneously.
Furthermore, it has been confirmed that by covering the heat generating cap as claimed in claim 3, the reaction at the time of straightening the hair is accelerated and the beautiful finish and the long-lasting effect of the hair dye last.

Claims (3) Translated from Japanese

システアミン塩酸塩又は１−チオグリセロールを３％以上１０％以下含有した還元剤を縮毛に塗布し水洗し縮毛矯正用ヘアーアイロンで毛髪を伸ばしたあと酸化染料を含有する染毛剤の第一剤と過酸化水素を含有する染毛剤第二剤の混合物で酸化し縮毛を直毛に矯正すると同時に染毛する縮毛矯正同時染毛方法。The first hair dye containing an oxidative dye after applying a reducing agent containing 3% or more and 10% or less of cysteamine hydrochloride or 1-thioglycerol to the curly hair, washing it with water and extending the hair with a curling iron for straightening hair. A method of simultaneous hair straightening, in which hair is oxidized with a mixture of a hair dye and a second hair dye containing hydrogen peroxide to straighten the curly hair and straighten at the same time. 染毛剤第一剤と染毛剤第二剤の混合物中の過酸化水素濃度が３％以上６％以下である請求項１の縮毛矯正同時染毛方法The method for simultaneously dyeing curly hair according to claim 1, wherein the hydrogen peroxide concentration in the mixture of the first hair dye and the second hair dye is 3% or more and 6% or less. システアミン塩酸塩又は１−チオグリセロールを含有した還元剤を縮毛に塗布し発熱キャップで頭髪を加温し頭髪を加温還元し水洗し縮毛矯正用ヘアーアイロンで毛髪を伸ばしたあと過酸化水素を含有する染毛剤の第一剤と第二剤の混合物で酸化し縮毛を自然な直毛すると同時に染毛する縮毛矯正同時染毛方法。Applying a reducing agent containing cysteamine hydrochloride or 1-thioglycerol to curly hair, warming the hair with a fever cap, warming and reducing the hair, washing with water, extending the hair with a curling hair straightener, and then hydrogen peroxide A method for simultaneously dyeing curly hair that is oxidized with a mixture of a first agent and a second agent of a hair dye containing hair to naturally straighten and simultaneously dye the curly hair.

JP2011087719A 2011-03-25 2011-03-25 Method of simultaneous straightening and dyeing of frizzy hair Withdrawn JP2012201679A (en) Priority Applications (1) Application Number Priority Date Filing Date Title JP2011087719A JP2012201679A (en) 2011-03-25 2011-03-25 Method of simultaneous straightening and dyeing of frizzy hair Applications Claiming Priority (1) Application Number Priority Date Filing Date Title JP2011087719A JP2012201679A (en) 2011-03-25 2011-03-25 Method of simultaneous straightening and dyeing of frizzy hair Publications (1) Family ID=47183023 Family Applications (1) Application Number Title Priority Date Filing Date JP2011087719A Withdrawn JP2012201679A (en) 2011-03-25 2011-03-25 Method of simultaneous straightening and dyeing of frizzy hair Country Status (1) Cited By (4) * Cited by examiner, † Cited by third party Publication number Priority date Publication date Assignee Title US9725771B2 (en) 2002-12-06 2017-08-08 Ibis Biosciences, Inc. Methods for rapid identification of pathogens in humans and animals US9752184B2 (en) 2001-03-02 2017-09-05 Ibis Biosciences, Inc. Methods for rapid forensic analysis of mitochondrial DNA and characterization of mitochondrial DNA heteroplasmy US9873906B2 (en) 2004-07-14 2018-01-23 Ibis Biosciences, Inc. Methods for repairing degraded DNA US9890408B2 (en) 2009-10-15 2018-02-13 Ibis Biosciences, Inc. Multiple displacement amplification Cited By (4) * Cited by examiner, † Cited by third party Publication number Priority date Publication date Assignee Title US9752184B2 (en) 2001-03-02 2017-09-05 Ibis Biosciences, Inc. Methods for rapid forensic analysis of mitochondrial DNA and characterization of mitochondrial DNA heteroplasmy US9725771B2 (en) 2002-12-06 2017-08-08 Ibis Biosciences, Inc. Methods for rapid identification of pathogens in humans and animals US9873906B2 (en) 2004-07-14 2018-01-23 Ibis Biosciences, Inc. Methods for repairing degraded DNA US9890408B2 (en) 2009-10-15 2018-02-13 Ibis Biosciences, Inc. Multiple displacement amplification Similar Documents Legal Events Date Code Title Description 2014-06-03 A300 Withdrawal of application because of no request for examination

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